Mapping of titanium particles in peri-implant oral mucosa by laser ablation inductively coupled plasma mass spectrometry and high-resolution optical darkfield microscopy

J Oral Pathol Med. 2011 May;40(5):412-20. doi: 10.1111/j.1600-0714.2010.00958.x. Epub 2010 Oct 24.

Abstract

The present study examines the quantity, size, element signatures and distribution of titanium particles in normal oral mucosal tissue and in oral mucosa exposed to a titanium implant. Tissue samples from six healthy patients were obtained by a full thickness biopsy taken from the edge of the oral mucosa when inserting a titanium dental implant. At the abutment insertion 6 months later, a punch test biopsy of oral mucosa was taken over the implant site. Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) is a sensitive and specific multi-element microanalytical technique that demonstrated the presence of Ti particles in the tissue adjacent to implant cover-screws. The epithelial part of the control samples revealed more particles than the corresponding area of the test samples, consisting partly of newly formed scar tissue. High-Resolution Optical Darkfield Microscope (HR-ODM) confirmed the presence of particles in both the control and the test samples. The combination of LA-ICP-MS and HR-ODM appears to be a powerful combination for detection of particles in oral tissues; optical microscopy provides an overview with histological references, whereas LA-ICP-MS identifies the chemical composition.

MeSH terms

  • Adult
  • Aged
  • Case-Control Studies
  • Dental Implantation, Endosseous
  • Dental Implants*
  • Female
  • Humans
  • Isotopes / analysis
  • Lasers, Solid-State
  • Limit of Detection
  • Logistic Models
  • Male
  • Microscopy / methods
  • Middle Aged
  • Mouth Mucosa / chemistry*
  • Particle Size
  • Plasma Gases
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / instrumentation
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / methods*
  • Titanium / analysis*

Substances

  • Dental Implants
  • Isotopes
  • Plasma Gases
  • Titanium