Characterisation and in vitro activities of surface attached dihydropyrrol-2-ones against Gram-negative and Gram-positive bacteria

Biofouling. 2010 Nov;26(8):913-21. doi: 10.1080/08927014.2010.531463.

Abstract

Bacterial infection of biomedical devices is still a major barrier to their use. This is compounded by increasing antibiotic resistance. Here, the specific covalent attachment of a series of dihydropyrrol-2-one (DHP), analogues of bacterial quorum sensing inhibitors, to surfaces via a Michael-type addition reaction is described. Differences in efficiency of attachment related to the substituent groups were found by X-ray photoelectron spectroscopy. The physical characteristics of the surfaces were further explored by atomic force microscopy and contact angle measurements. The ability of these coatings to prevent the formation of a biofilm by Pseudomonas aeruginosa and Staphylococcus aureus was examined using confocal laser scanning microscopy and image analysis. The DHP-treated surfaces showed significant reductions in bacterial adhesion without increased killing for both strains of bacteria (p < 0.001). 5-Methylene-1-(prop-2-enoyl)-4-phenyl-dihydropyrrol-2-one was identified as having broad spectrum activity and consequently represents an excellent candidate for the development of novel surfaces for the prevention of biomedical device infections.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Anti-Bacterial Agents / chemistry
  • Anti-Bacterial Agents / pharmacology*
  • Bacterial Adhesion / drug effects
  • Biofilms / drug effects
  • Biofouling*
  • Microbial Sensitivity Tests
  • Microscopy, Atomic Force
  • Photoelectron Spectroscopy
  • Pseudomonas aeruginosa / drug effects*
  • Pseudomonas aeruginosa / physiology
  • Pyrrolidinones / chemistry
  • Pyrrolidinones / pharmacology*
  • Quorum Sensing / drug effects*
  • Staphylococcus aureus / drug effects*
  • Staphylococcus aureus / physiology
  • Surface Properties

Substances

  • 5-methylene-1-(prop-2-enoyl)-4-phenyldihydropyrrol-2-one
  • Anti-Bacterial Agents
  • Pyrrolidinones