Microtiter plate quantification of mutant and wild-type huntingtin normalized to cell count

Anal Biochem. 2011 Mar 15;410(2):304-6. doi: 10.1016/j.ab.2010.11.044. Epub 2010 Dec 4.

Abstract

Huntington's disease is caused by a gain-of-function neurotoxic mutation in normally neuroprotective huntingtin. Sensitive assays are required to discriminate mutant huntingtin from wild-type huntingtin. We have developed a normalized 384-plate assay for determination of mutant and wild-type huntingtin. Based on a single pipetting step, the sensitive assay uses two antibody pairs for simultaneous mutant and wild-type huntingtin time-resolved fluorescence resonance energy transfer detection combined with PicoGreen quantification of double-stranded DNA. The assay can be used for discovery of drugs reducing mutant huntingtin over wild-type huntingtin and for assessing the value of huntingtin as a disease progression marker, and it is adaptable to other proteins of interest.

MeSH terms

  • Antibodies / analysis*
  • Cell Count
  • Cell Line
  • DNA
  • Fibroblasts / cytology
  • Fluorescence Resonance Energy Transfer / methods*
  • Humans
  • Huntingtin Protein
  • Huntington Disease / genetics
  • Mutant Proteins / analysis*
  • Mutant Proteins / chemistry*
  • Nerve Tissue Proteins / analysis*
  • Nerve Tissue Proteins / chemistry*
  • Nuclear Proteins / analysis*
  • Nuclear Proteins / chemistry*
  • Organic Chemicals

Substances

  • Antibodies
  • HTT protein, human
  • Huntingtin Protein
  • Mutant Proteins
  • Nerve Tissue Proteins
  • Nuclear Proteins
  • Organic Chemicals
  • PicoGreen
  • DNA