The binding specificity of the marker antibodies Tra-1-60 and Tra-1-81 reveals a novel pluripotency-associated type 1 lactosamine epitope

Glycobiology. 2011 Sep;21(9):1125-30. doi: 10.1093/glycob/cwq209. Epub 2010 Dec 15.

Abstract

The expression of the epitopes recognized by the monoclonal antibodies Tra-1-60 and Tra-1-81 is routinely used to assess the pluripotency status of human embryonic stem cells (hESCs) and induced pluripotent stem (iPS) cells. Although it is known that the epitopes recognized by Tra-1-60 and Tra-1-81 are carbohydrates, the exact molecular identity of these epitopes has been unclear. Glycan array analysis with more than 500 oligosaccharide structures revealed specific binding of Tra-1-60 and Tra-1-81 to two molecules containing terminal type 1 lactosamine: Galβ1-3GlcNAcβ1-3Galβ1-4GlcNAc and Galβ1-3GlcNAcβ1-3Galβ1-4GlcNAcβ1-6(Galβ1-3GlcNAcβ1-3)Galβ1-4Glc. The type 1 disaccharide in itself was not sufficient for binding, indicating that the complete epitope requires an extended tetrasaccharide structure where the type 1 disaccharide is β1,3-linked to type 2 lactosamine. Our mass spectrometric analysis complemented with glycosidase digestions of hESC O-glycans indicated the presence of the extended tetrasaccharide epitope on an O-glycan with the likely structure Galβ1-3GlcNAcβ1-3Galβ1-4GlcNAcβ1-6(Galβ1-3)GalNAc. Thus, the present data indicate that the pluripotency marker antibodies Tra-1-60 and Tra-1-81 recognize the minimal epitope Galβ1-3GlcNAcβ1-3Galβ1-4GlcNAc, which is present in hESCs as a part of a mucin-type O-glycan structure. The exact molecular identity of Tra-1-60 and Tra-1-81 is important for the development of improved tools to characterize the pluripotent phenotype.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Sugars* / chemistry
  • Amino Sugars* / immunology
  • Antibodies / immunology
  • Antibodies / metabolism*
  • Antibody Specificity
  • Binding Sites
  • Biomarkers / analysis
  • Carbohydrate Conformation
  • Carbohydrate Sequence
  • Embryonic Stem Cells / cytology
  • Embryonic Stem Cells / immunology
  • Embryonic Stem Cells / metabolism*
  • Epitopes* / chemistry
  • Epitopes* / immunology
  • Flow Cytometry
  • Glycoside Hydrolases / metabolism
  • Humans
  • Mass Spectrometry
  • Molecular Sequence Data
  • Oligosaccharides / chemistry*
  • Oligosaccharides / immunology
  • Pluripotent Stem Cells / cytology
  • Pluripotent Stem Cells / immunology
  • Pluripotent Stem Cells / metabolism*
  • Protein Binding

Substances

  • Amino Sugars
  • Antibodies
  • Biomarkers
  • Epitopes
  • Oligosaccharides
  • lactosamine
  • Glycoside Hydrolases