Using azobenzene incorporated DNA aptamers to probe molecular binding interactions

Bioconjug Chem. 2011 Feb 16;22(2):282-8. doi: 10.1021/bc100402p. Epub 2011 Jan 19.

Abstract

The rational design of DNA/RNA aptamers for use as molecular probes depends on a clear understanding of their structural elements in relation to target-aptamer binding interactions. We present a simple method to create aptamer probes that can occupy two different structural states. Then, based on the difference in binding affinity between these states, target-aptamer binding interactions can be elucidated. The basis of our two-state system comes from the incorporation of azobenzene within the DNA strand. Azobenzene can be used to photoregulate the melting of DNA-duplex structures. When incorporated into aptamers, the light-regulated conformational change of azobenzene can be used to analyze how aptamer secondary structure is involved in target binding. Azobenzene-modified aptamers showed no change in target selectivity, but showed differences in binding affinity as a function of the number, position, and conformation of azobenzene modifications. Aptamer probes that can change binding affinity on demand may have future uses in targeted drug delivery and photodynamic therapy.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Aptamers, Nucleotide / chemical synthesis
  • Aptamers, Nucleotide / chemistry*
  • Aptamers, Nucleotide / metabolism*
  • Azo Compounds / chemical synthesis
  • Azo Compounds / chemistry*
  • Azo Compounds / metabolism
  • Binding Sites
  • Flow Cytometry
  • Humans
  • Light
  • Molecular Probes / chemical synthesis
  • Molecular Probes / chemistry*
  • Molecular Probes / metabolism*
  • Molecular Structure
  • Stereoisomerism
  • Tumor Cells, Cultured

Substances

  • Aptamers, Nucleotide
  • Azo Compounds
  • Molecular Probes
  • azobenzene