New subfragment 1 of skeletal muscle myosin obtained by thrombin cleavage

Biochemistry. 1990 Feb 20;29(7):1840-6. doi: 10.1021/bi00459a025.

Abstract

The head of the myosin molecule (i.e., subfragment 1 with a heavy chain of 95 kDa) is usually obtained by chymotryptic cleavage in the presence of a divalent cation chelator. In the present work, we used another specific proteolytic enzyme, thrombin, to produce a limited cut within the myosin molecule, resulting in a new species of N-terminal fragment. Treatment of skeletal muscle myosin yielded a 97-kDa split heavy chain associated with intact light chains, corresponding to a single cut. The ATPase activities of this new S-1 derivative were slightly affected by the breakdown. It recognized actin in an ATP-dependent manner, as expected, with an affinity 2-5 times higher than that of the usual chymotryptic S-1 preparation but with a very different electron microscopic pattern. Functional differences are noted, and we involve them more precisely in relation to possible structural aspects of the additional C-terminal segment extending the usual S-1 heavy chain from 95 to 97 kDa.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Actins / ultrastructure
  • Amino Acid Sequence
  • Animals
  • Arginase
  • Chymotrypsin / metabolism
  • Fluorescent Dyes
  • Humans
  • Microscopy, Electron
  • Molecular Sequence Data
  • Molecular Weight
  • Muscles / metabolism
  • Myosin Subfragments / isolation & purification*
  • Myosin Subfragments / metabolism
  • Myosin Subfragments / ultrastructure
  • Myosins / isolation & purification
  • Myosins / metabolism
  • Naphthalenesulfonates
  • Rabbits
  • Scattering, Radiation
  • Sequence Homology, Nucleic Acid
  • Thrombin* / metabolism

Substances

  • Actins
  • Fluorescent Dyes
  • Myosin Subfragments
  • Naphthalenesulfonates
  • 1,5-I-AEDANS
  • Chymotrypsin
  • Thrombin
  • Arginase
  • Myosins