A miniature cell has been designed and constructed to measure gas solubility in crude oils and bitumen. The cell was made of stainless steel with a total internal volume of 1.835 cc and only an oil sample of 0.4 cc was required for one set of measurements at different pressures. By using this small cell, the waiting time for reaching equilibrium was less than 10 min. The technique was validated by measuring CO(2) gas solubility in two bitumen samples. The results were compared and found to be in very good agreement with available data. The apparatus was also used to study the effect of ashphaltene on CO(2) solubility in bitumen. It was shown that ashphaltene had a negligible effect on CO(2) solubility in bitumen.