Application of magnetic particles modified with amino groups to adsorb copper ions in aqueous solution

J Environ Sci (China). 2011;23(1):44-50. doi: 10.1016/s1001-0742(10)60371-3.

Abstract

A magnetic adsorbent can be easily recovered from treated water by magnetic force, without requiring further downstream treatment. In this research, amine-functionalized silica magnetite has been synthesized using N-[3-(trimethoxysilyl)propyl]-ethylenediamine (TPED) as a surface modification agent. The synthesized magnetic amine adsorbents were used to adsorb copper ions in an aqueous solution in a batch system, and the maximum adsorption was found to occur at pH 5.5 +/- 0.1. The adsorption equilibrium data fitted the Langmuir isotherm equation reasonably well, with a maximum adsorption capacity of 10.41 mg/g. A pseudo second-order model could best describe the adsorption kinetics, and the derived activation energy was 26.92 kJ/mol. The optimum condition to desorb Cu2+ from NH2/SiO2/Fe3O4 was provided by a solution with 0.1 mol/L HNO3.

MeSH terms

  • Adsorption
  • Amines / chemistry*
  • Copper / chemistry*
  • Hydrogen-Ion Concentration
  • Ions
  • Kinetics
  • Magnetics / methods*
  • Models, Chemical
  • Particulate Matter / chemistry*
  • Solutions
  • Spectrophotometry, Ultraviolet
  • Spectroscopy, Fourier Transform Infrared
  • Temperature
  • X-Ray Diffraction

Substances

  • Amines
  • Ions
  • Particulate Matter
  • Solutions
  • Copper