Femtosecond nanocrystallography using X-ray lasers for membrane protein structure determination

Curr Opin Struct Biol. 2011 Aug;21(4):509-16. doi: 10.1016/j.sbi.2011.06.001.

Abstract

The invention of free electron X-ray lasers has opened a new era for membrane protein structure determination with the recent first proof-of-principle of the new concept of femtosecond nanocrystallography. Structure determination is based on thousands of diffraction snapshots that are collected on a fully hydrated stream of nanocrystals. This review provides a summary of the method and describes how femtosecond X-ray crystallography overcomes the radiation-damage problem in X-ray crystallography, avoids the need for growth and freezing of large single crystals while offering a new method for direct digital phase determination by making use of the fully coherent nature of the X-ray beam. We briefly review the possibilities for time-resolved crystallography, and the potential for making 'molecular movies' of membrane proteins at work.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.
  • Review

MeSH terms

  • Crystallography, X-Ray / methods*
  • Humans
  • Injections
  • Lasers* / adverse effects
  • Membrane Proteins / chemistry*
  • Nanotechnology / methods*

Substances

  • Membrane Proteins