An allenic Pauson-Khand approach to 6,12-guaianolides

Org Lett. 2011 Dec 2;13(23):6304-7. doi: 10.1021/ol2028515. Epub 2011 Nov 9.

Abstract

Cyclocarbonylation of α-methylene butyrolactone-containing allene-ynes affords 6,12-guaianolide ring systems. Incorporation of the α-methylene butyrolactone early in a synthetic sequence is rare for reactivity reasons; however, this moiety proves to be beneficial to the allenic Pauson-Khand reaction. The three double bonds and the ketone in the resulting 5-7-5 ring system bear significant differences in their reactivity and are ideally positioned for synthetic application to 6,12-guaianolides and analogs.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • 4-Butyrolactone / analogs & derivatives
  • 4-Butyrolactone / chemistry*
  • Alkadienes / chemistry*
  • Alkynes / chemistry*
  • Catalysis
  • Combinatorial Chemistry Techniques
  • Molecular Structure
  • Sesquiterpenes, Guaiane / chemical synthesis*
  • Sesquiterpenes, Guaiane / chemistry

Substances

  • Alkadienes
  • Alkynes
  • Sesquiterpenes, Guaiane
  • 4-Butyrolactone