Rapid access to conformational analogues of (+)-peloruside A

Org Lett. 2012 Feb 3;14(3):669-71. doi: 10.1021/ol203268t. Epub 2012 Jan 11.

Abstract

An efficient synthetic strategy for rapid access to analogues of peloruside A has been demonstrated. The synthetic route was highlighted by a simple esterification-based fragment coupling and a late stage ring-closing metathesis reaction. This convergent route has provided access to rationally designed analogues inspired by the solution conformational preferences of peloruside A.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Bridged Bicyclo Compounds, Heterocyclic / chemistry*
  • Lactones / chemistry*
  • Macrolides / chemistry
  • Molecular Conformation
  • Time Factors

Substances

  • Bridged Bicyclo Compounds, Heterocyclic
  • Lactones
  • Macrolides
  • peloruside A
  • peloruside B