Synthesis and structure of distanna and tristanna ansa half-sandwich complexes of ruthenium and nickel

Inorg Chem. 2012 Feb 6;51(3):1225-7. doi: 10.1021/ic202512y. Epub 2012 Jan 13.

Abstract

The synthesis and structural characterization of the first tin-bridged ansa half-sandwich complexes via a two-step protocol from Na[η(5)-C(5)H(5)Ru(CO)(2)] and in situ generated Na[η(5)-C(5)H(5)Ni(CO)] are presented. Both compounds are characterized by multinuclear NMR spectroscopy and single-crystal diffraction.

MeSH terms

  • Crystallography, X-Ray
  • Magnetic Resonance Spectroscopy
  • Models, Molecular
  • Nickel / chemistry*
  • Ruthenium Compounds / chemical synthesis
  • Ruthenium Compounds / chemistry*

Substances

  • Ruthenium Compounds
  • Nickel