[Determination of loganin in Pterocephalus hookeri by HPLC]

Zhongguo Zhong Yao Za Zhi. 2011 Dec;36(24):3472-4.
[Article in Chinese]

Abstract

Objective: To develop an HPLC method for determination of loganin in Pterocephalus hookeri.

Method: The analysis was performed on a Welchrom C18 column (4.6 mm x 250 mm, 5 microm) with acetonitrile-water (12:88) as the the mobile phase at a flow rate of 1 mL x min(-1) and the detection wavelength was 240 nm.

Result: The peak areas and injection amounts of loganin had a good linear relationship at the range of 0.06-1.2 microg. The average recovery was 97.0%, and the RSD was 1.4%.

Conclusion: The method is simple, accurate, and can be used for its quality control.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Chromatography, High Pressure Liquid / methods*
  • Iridoids / analysis*
  • Medicine, Tibetan Traditional*
  • Plants, Medicinal / chemistry*

Substances

  • Iridoids
  • loganin