Photopatterning of multilayer n-alkylsilane films

Langmuir. 2012 May 8;28(18):7129-33. doi: 10.1021/la3011579. Epub 2012 Apr 23.

Abstract

Surface photopatterning of organosilane self-assembled monolayers (SAM) has received increasing attention since its introduction 20 years ago. Herein we report for the first time a cost-efficient soft photopatterning technique affording amplified 3D multilayer structures. The essential chemistry relies on a spatially controlled photoacid-catalyzed hydrolysis and polycondensation of n-alkyltrimethoxysilane precursors (n-C(12)H(25)Si(OCH(3))(3),). Amphiphilic siloxane species are photogenerated locally and are able to self-assemble spontaneously into a long-range-ordered lamellar mesostructure.

MeSH terms

  • Membranes, Artificial*
  • Particle Size
  • Photochemical Processes
  • Silanes / chemistry*
  • Surface Properties

Substances

  • Membranes, Artificial
  • Silanes