Microwave-assisted direct liquefaction of Ulva prolifera for bio-oil production by acid catalysis

Bioresour Technol. 2012 Jul:116:133-9. doi: 10.1016/j.biortech.2012.04.036. Epub 2012 Apr 21.

Abstract

Production of bio-oil by microwave-assisted direct liquefaction (MADL) of Ulva prolifera was investigated, and the bio-oil was analyzed by elementary analysis, Fourier transform infrared spectroscopic analysis (FT-IR), and gas chromatography-mass spectrometry (GC-MS). The results indicate that the liquefaction yield is influenced by the microwave power, liquefaction temperature, liquefaction time, catalyst content, solvent-to-feedstock ratio and moisture content. The maximum liquefaction yield of U. prolifera (moisture content of 8%) was 84.81%, which was obtained under microwave power of 600 W for 30 min at 180 °C with solvent-to-feedstock ratio of 16:1 and 6% H(2)SO(4). The bio-oil was composed of benzenecarboxylic acid, diethyl phthalate, long-chain fatty acids (C(13) to C(18)), fatty acid methyl esters and water. The results suggest that U. prolifera is a viable eco-friendly, green feedstock substitute for biofuels and chemicals production.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Acids / chemistry*
  • Biofuels / analysis*
  • Biomass
  • Biotechnology / methods*
  • Catalysis
  • Gas Chromatography-Mass Spectrometry
  • Hot Temperature
  • Humidity
  • Microwaves*
  • Plant Oils / chemical synthesis*
  • Solvents / chemistry
  • Spectroscopy, Fourier Transform Infrared
  • Time Factors
  • Ulva / chemistry*

Substances

  • Acids
  • Biofuels
  • Plant Oils
  • Solvents