Biochemical and structural characterization of the complex agarolytic enzyme system from the marine bacterium Zobellia galactanivorans

J Biol Chem. 2012 Aug 31;287(36):30571-84. doi: 10.1074/jbc.M112.377184. Epub 2012 Jul 9.

Abstract

Zobellia galactanivorans is an emerging model bacterium for the bioconversion of algal biomass. Notably, this marine Bacteroidetes possesses a complex agarolytic system comprising four β-agarases and five β-porphyranases, all belonging to the glycoside hydrolase family 16. Although β-agarases are specific for the neutral agarobiose moieties, the recently discovered β-porphyranases degrade the sulfated polymers found in various quantities in natural agars. Here, we report the biochemical and structural comparison of five β-porphyranases and β-agarases from Z. galactanivorans. The respective degradation patterns of two β-porphyranases and three β-agarases are analyzed by their action on defined hybrid oligosaccharides. In light of the high resolution crystal structures, the biochemical results allowed a detailed mapping of substrate specificities along the active site groove of the enzymes. Although PorA displays a strict requirement for C6-sulfate in the -2- and +1-binding subsites, PorB tolerates the presence of 3-6-anhydro-l-galactose in subsite -2. Both enzymes do not accept methylation of the galactose unit in the -1 subsite. The β-agarase AgaD requires at least four consecutive agarose units (DP8) and is highly intolerant to modifications, whereas for AgaB oligosaccharides containing C6-sulfate groups at the -4, +1, and +3 positions are still degraded. Together with a transcriptional analysis of the expression of these enzymes, the structural and biochemical results allow proposition of a model scheme for the agarolytic system of Z. galactanivorans.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Agar / chemistry*
  • Bacterial Proteins / chemistry*
  • Crystallography, X-Ray
  • Flavobacteriaceae / enzymology*
  • Glycoside Hydrolases / chemistry*
  • Models, Molecular*
  • Protein Structure, Tertiary
  • Structure-Activity Relationship

Substances

  • Bacterial Proteins
  • Agar
  • Glycoside Hydrolases
  • agarase

Associated data

  • PDB/4ASM
  • PDB/4ATE
  • PDB/4ATF