Optimization and proficiency testing of a pseudovirus-based assay for detection of HIV-1 neutralizing antibody in China

J Virol Methods. 2012 Nov;185(2):267-75. doi: 10.1016/j.jviromet.2012.07.011. Epub 2012 Jul 13.

Abstract

Among the neutralizing antibody evaluation assays, the single-cycle pseudovirus infection assay is high-throughput and can provide rapid, sensitive and reproducible measurements after a single cycle of infection. Cell counts, pseudovirus inoculation levels, amount of diethylaminoethyl-dextran (DEAE-dextran), and the nonspecific effects of serum and plasma were tested to identify the optimal conditions for a neutralizing antibody assay based on pseudoviruses. Optimal conditions for cell counts, pseudovirus inoculation, and amount of DEAE-dextran were 1 × 10(4)cells/well, 200TCID(50)/well, and 15 μg/ml, respectively. Compared with serum samples, high-concentration anticoagulants reduced the relative light unit (RLU) value. The RLU value increased sharply initially but then decreased slowly with dilution of the plasma sample. Test kits containing 10 HIV-1 CRF07/08_BC pseudovirus strains and 10 plasma samples from individuals infected with HIV-1 CRF07/08_BC were assembled into two packages and distributed to nine laboratories with a standard operating procedure included. For the 10 laboratories that evaluated the test, 17 of 44 (37%) laboratory pairs were considered equivalent. A statistical qualification rule was developed based on the testing results from 5 experienced laboratories, where a laboratory qualified if at least 83% of values lied within the acceptable range.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antibodies, Neutralizing / blood*
  • Antibodies, Neutralizing / immunology
  • Cell Count
  • Cell Line
  • China
  • Cytopathogenic Effect, Viral
  • DEAE-Dextran / chemistry
  • HIV Antibodies / blood*
  • HIV Antibodies / immunology
  • HIV Infections / diagnosis*
  • HIV Infections / immunology
  • HIV Infections / virology
  • HIV-1 / immunology
  • HIV-1 / isolation & purification*
  • HIV-1 / pathogenicity
  • Humans
  • Inhibitory Concentration 50
  • Laboratory Proficiency Testing / methods
  • Laboratory Proficiency Testing / standards*
  • Neutralization Tests / methods*
  • Neutralization Tests / standards
  • Reagent Kits, Diagnostic / standards
  • Reproducibility of Results
  • Sensitivity and Specificity

Substances

  • Antibodies, Neutralizing
  • HIV Antibodies
  • Reagent Kits, Diagnostic
  • DEAE-Dextran