Synthesis of stable genipin derivatives and studies of their neuroprotective activity in PC12 cells

ChemMedChem. 2012 Sep;7(9):1661-8. doi: 10.1002/cmdc.201200258. Epub 2012 Jul 30.

Abstract

Modifications at C1, C7, C8, and C10 of genipin were conducted, and the neurotrophic effects of all derivatives were studied. Genipin derivatives 1-4 were obtained in mild to high yield. Compounds 1 and 4 are more stable than genipin if exposed to nucleophiles. All the derivatives display higher neurotrophic activities than genipin. Compound 4 is the most active, with the least optimal dose. Both genipin and 4 up-regulated the activity of nNOS in PC12 cells. The effect of 4 is inhibited not only by 7-NI, a specific inhibitor of nNOS, but also by L-NIO, a specific inhibitor of eNOS; in the case of genipin, its effect is only inhibited by 7-NI. All the results indicate that 4 is a promising lead compound for the development of new drugs in the treatment of neurodegenerative diseases with the ability to address multiple drug targets.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Cell Survival / drug effects
  • Gardenia / chemistry
  • Iridoids / chemical synthesis*
  • Iridoids / chemistry
  • Iridoids / pharmacology*
  • Neurons / drug effects*
  • Neurons / enzymology
  • Neuroprotective Agents / chemical synthesis*
  • Neuroprotective Agents / chemistry
  • Neuroprotective Agents / pharmacology*
  • Nitric Oxide Synthase Type I / antagonists & inhibitors
  • Nitric Oxide Synthase Type I / metabolism
  • Nitric Oxide Synthase Type III / antagonists & inhibitors
  • Nitric Oxide Synthase Type III / metabolism
  • PC12 Cells
  • Rats

Substances

  • Iridoids
  • Neuroprotective Agents
  • gardenamide A
  • genipin
  • Nitric Oxide Synthase Type I
  • Nitric Oxide Synthase Type III