Human IgA-binding peptides selected from random peptide libraries: affinity maturation and application in IgA purification

J Biol Chem. 2012 Dec 14;287(51):43126-36. doi: 10.1074/jbc.M112.389742. Epub 2012 Oct 17.

Abstract

Phage display system is a powerful tool to design specific ligands for target molecules. Here, we used disulfide-constrained random peptide libraries constructed with the T7 phage display system to isolate peptides specific to human IgA. The binding clones (A1-A4) isolated by biopanning exhibited clear specificity to human IgA, but the synthetic peptide derived from the A2 clone exhibited a low specificity/affinity (K(d) = 1.3 μm). Therefore, we tried to improve the peptide using a partial randomized phage display library and mutational studies on the synthetic peptides. The designed Opt-1 peptide exhibited a 39-fold higher affinity (K(d) = 33 nm) than the A2 peptide. An Opt-1 peptide-conjugated column was used to purify IgA from human plasma. However, the recovered IgA fraction was contaminated with other proteins, indicating nonspecific binding. To design a peptide with increased binding specificity, we examined the structural features of Opt-1 and the Opt-1-IgA complex using all-atom molecular dynamics simulations with explicit water. The simulation results revealed that the Opt-1 peptide displayed partial helicity in the N-terminal region and possessed a hydrophobic cluster that played a significant role in tight binding with IgA-Fc. However, these hydrophobic residues of Opt-1 may contribute to nonspecific binding with other proteins. To increase binding specificity, we introduced several mutations in the hydrophobic residues of Opt-1. The resultant Opt-3 peptide exhibited high specificity and high binding affinity for IgA, leading to successful isolation of IgA without contamination.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Motifs
  • Amino Acid Sequence
  • Amino Acid Substitution
  • Antibody Affinity / immunology*
  • Chromatography, Affinity
  • Conserved Sequence
  • Enzyme-Linked Immunosorbent Assay
  • Humans
  • Immunoglobulin A / chemistry
  • Immunoglobulin A / isolation & purification*
  • Immunoglobulin A / metabolism*
  • Molecular Dynamics Simulation
  • Molecular Sequence Data
  • Mutation / genetics
  • Peptide Library*
  • Peptides / chemistry
  • Peptides / metabolism*
  • Protein Binding
  • Receptors, Fc / chemistry
  • Reproducibility of Results
  • Sequence Homology, Amino Acid
  • Thermodynamics

Substances

  • Immunoglobulin A
  • Peptide Library
  • Peptides
  • Receptors, Fc