Sagittal focusing of synchrotron radiation X-rays using a winged crystal

J Synchrotron Radiat. 2013 Mar;20(Pt 2):219-25. doi: 10.1107/S0909049512049813. Epub 2013 Jan 23.

Abstract

A Si(111) winged crystal has been designed to minimize anticlastic bending and improve sagittal focusing efficiency. The crystal was thin with wide stiffening wings. The length-to-width ratio of the crystal was optimized by finite element analysis, and the optimal value was larger than the `golden value'. The analysis showed that the slope error owing to anticlastic bending is less than the Darwin width. The X-rays were focused two-dimensionally using the crystal and a tangentially bent mirror. The observed profiles of the focal spot agreed well with the results of a ray-tracing calculation in the energy range from 8 to 17.5 keV. X-ray diffraction measurements with a high signal-to-noise ratio using this focusing system were demonstrated for a small protein crystal.

Keywords: SPring-8; crystal bender; double-crystal monochromator; sagittal focusing; two-dimensional focusing; winged crystal.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Crystallization / instrumentation
  • Equipment Design
  • Muramidase / chemistry*
  • Synchrotrons
  • X-Ray Diffraction / methods*

Substances

  • Muramidase