Synthesis and biological evaluation of fluoro analogues of antimitotic phenstatin

Bioorg Med Chem. 2013 Jun 1;21(11):2932-40. doi: 10.1016/j.bmc.2013.03.064. Epub 2013 Apr 4.

Abstract

With the aim of investigating the influence of fluorine, in particular on the A-ring, a new series of fluoro analogues (7a-l) of phenstatin (3) was synthesized and tested for interactions with tubulin polymerization and evaluated for cytotoxicity on an NCI-60 human cancer cell lines panel. We have shown that the replacement of 3,4,5-trimethoxyphenyl A-ring of phenstatin with 2,4,5-trifluoro-3-methoxyphenyl unit, results in the conservation of both antitubulin and cytotoxic effect. Fluoro isocombretastatin 7k was the most effective anticancer agent in the present study and demonstrated the highest antiproliferative potential on leukemia cell lines SR (GI50=15 nM) and HL-60(TB) (GI50=23 nM) and on melanoma cell line MDA-MB-435 (GI50=19 nM).

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antimitotic Agents / chemical synthesis*
  • Antimitotic Agents / pharmacology
  • Antineoplastic Agents / chemical synthesis*
  • Antineoplastic Agents / pharmacology
  • Benzophenones / chemical synthesis*
  • Benzophenones / pharmacology
  • Cell Line, Tumor
  • Cell Survival / drug effects
  • Fluorine Compounds / chemical synthesis*
  • Fluorine Compounds / pharmacology
  • Halogenation
  • Humans
  • Inhibitory Concentration 50
  • Mitosis / drug effects
  • Organophosphates / chemical synthesis*
  • Organophosphates / pharmacology
  • Prodrugs / chemical synthesis*
  • Prodrugs / pharmacology

Substances

  • Antimitotic Agents
  • Antineoplastic Agents
  • Benzophenones
  • Fluorine Compounds
  • Organophosphates
  • Prodrugs
  • phenstatin phosphate