Heterologous expression and biochemical characterization of an endo-β-1,4-glucanase from Thermobifida fusca

Biotechnol Appl Biochem. 2013 May-Jun;60(3):348-55. doi: 10.1002/bab.1097. Epub 2013 Apr 30.

Abstract

The endoglucanase Cel5A from Thermobifida fusca was cloned and expressed in Escherichia coli BL21(DE3). The carboxymethyl cellulase (CMCase) activity in shake flasks and 3-L fermentation scale reached 46.8 and 656.6 IU/mL, respectively. The CMCase activity in 3-L fermentation scale represented the highest yield of T. fusca Cel5A reported so far. Recombinant Cel5A was purified and characterized in detail. The optimum temperature of recombinant enzyme was 80 °C, and the half-life of the enzyme was 132 H at 50 °C and 65 H at 60 °C. The activity of recombinant Cel5A was retained more than 90% over the range of pH 5.0-10.0 with maximal activity at pH 5.5. Using carboxymethyl cellulose as the substrate, the Km and Vmax values were 5.1 mg/mL and 48.7 IU/mg, respectively. The enzyme showed superstability in surfactants and was retained above 90% activity after treatment with sodium dodecyl sulfate, linear alkyl benzene sulfonate, fatty alcohol polyoxyethylene (9) ether, and polyoxyethylene (10) nonyl phenyl ether at 25 °C for 1 H, indicating that the enzyme could be a valuable component in detergents. The potential mechanism of this stability was investigated by analysis of the electrostatic potential of the surface of the enzyme.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Actinomycetales / enzymology
  • Actinomycetales / genetics*
  • Actinomycetales / metabolism*
  • Cellulase / genetics*
  • Cellulase / metabolism*
  • Cloning, Molecular / methods
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Fermentation / genetics
  • Half-Life
  • Hydrogen-Ion Concentration
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Temperature

Substances

  • Recombinant Proteins
  • endoglucanase Cel5A
  • Cellulase