Solvent-manipulated guest binding and signaling of a fluorescent resorcin[4]arene cavitand with 1,3,2-benzodiazaboryl D-π-A conjugation flaps

J Org Chem. 2013 Jun 7;78(11):5782-7. doi: 10.1021/jo4006238. Epub 2013 May 21.

Abstract

The conformation of resorcin[4]arene cavitand system 1 was controlled by DMSO through a hydrogen bonding network between benzodiazaborole NHs of the cavitand flaps and DMSO molecules to stabilize the vase form. Subsequently, a guest-binding cavity of 1 was formed to accommodate tetraalkylammonium guest 3, permitting the monitoring of the guest by the unaided eye as a result of a CH-π interaction between the benzodiazaborole π-donor group and the guest.

MeSH terms

  • Aza Compounds / chemistry*
  • Boron Compounds / chemistry*
  • Calixarenes / chemistry*
  • Fluorescence*
  • Hydrogen Bonding
  • Molecular Structure
  • Phenylalanine / analogs & derivatives*
  • Phenylalanine / chemistry
  • Solvents / chemistry

Substances

  • Aza Compounds
  • Boron Compounds
  • Solvents
  • resorcinarene
  • Calixarenes
  • Phenylalanine