A novel ∼34-kDa α-amylase from psychrotroph Exiguobacterium sp. SH3: production, purification, and characterization

Biotechnol Appl Biochem. 2014 Mar-Apr;61(2):118-25. doi: 10.1002/bab.1140. Epub 2013 Nov 14.

Abstract

An amylase-producing psychrotroph bacterium was isolated from soil and identified as belonging to the genus Exiguobacterium. A novel cold-adapted α-amylase, Amy SH3, was purified from culture medium of this bacterium using acetone precipitation and DEAE-Sepharose anion-exchange chromatography. The molecular mass of the enzyme was estimated about 34 kDa using SDS-PAGE. Biochemical characterization of Amy SH3 revealed that the optimum temperature for maximum activity of Amy SH3 was 37°C. However, Amy SH3 was also active at cold temperatures, showing 13% and 39% activity at 0 and 10°C, respectively. The optimum pH for maximum activity of Amy SH3 was pH 7, whereas the amylase was active over a pH range of 5 to 10. The activity of Amy SH3 was enhanced by Co²⁺ but decreased by Mg²⁺, Mn²⁺, Zn²⁺, Fe²⁺, and Ca²⁺. Amy SH3 was able to retain 76% of its activity in the presence of 0.5% SDS. The K(m) and V(max) of the enzyme were calculated to be 0.06 mg/mL and 4,010 U/mL, respectively. The cold-adapted Amy SH3 seems very promising for applications at ambient temperature.

Keywords: Exiguobacterium; characterization; psychrotroph; purification; α-amylase.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacillales / enzymology*
  • Chromatography, Ion Exchange
  • Culture Media
  • Electrophoresis, Polyacrylamide Gel
  • Hydrogen-Ion Concentration
  • Kinetics
  • Molecular Weight
  • Temperature
  • alpha-Amylases / biosynthesis*
  • alpha-Amylases / chemistry*
  • alpha-Amylases / genetics
  • alpha-Amylases / isolation & purification*

Substances

  • Culture Media
  • alpha-Amylases