Design, synthesis and biological evaluation of some 2-azetidinone derivatives as potential antihyperlipidemic agents

Arch Pharm (Weinheim). 2013 Dec;346(12):872-81. doi: 10.1002/ardp.201300262. Epub 2013 Oct 20.

Abstract

In an effort to develop new molecules with improved antihyperlipidemic activity, eight new 2-azetidinone analogs (4a-4h) of ezetimibe were designed through in silico docking experiments with the crystal structure of the Niemann-Pick C1-like 1 protein (NPC1L1). Synthesis and further antihyperlipdemic evaluation of this series in the Triton WR 1339 induced hyperlipidemic rat model showed some of the molecules to exhibit significant lipid-lowering effects comparable to ezetimibe. Correlation between the observed biological activity and the in silico molecular docking scores of the compounds was observed.

Keywords: 2-Azetidinone; Antihyperlipidemic; Ezetimibe; Molecular docking; NPC1L1.

Publication types

  • Comparative Study

MeSH terms

  • Animals
  • Azetidines / chemical synthesis*
  • Azetidines / metabolism
  • Azetidines / pharmacology*
  • Binding Sites
  • Biomarkers / blood
  • Crystallography, X-Ray
  • Disease Models, Animal
  • Drug Design*
  • Ezetimibe
  • Female
  • Hyperlipidemias / blood
  • Hyperlipidemias / chemically induced
  • Hyperlipidemias / drug therapy*
  • Hypolipidemic Agents / chemical synthesis*
  • Hypolipidemic Agents / metabolism
  • Hypolipidemic Agents / pharmacology*
  • Lipids / blood
  • Male
  • Membrane Proteins / chemistry
  • Membrane Proteins / metabolism
  • Membrane Transport Proteins
  • Models, Molecular
  • Molecular Docking Simulation
  • Molecular Structure
  • Polyethylene Glycols
  • Protein Conformation
  • Rats
  • Rats, Wistar

Substances

  • 2-azetidinone
  • Azetidines
  • Biomarkers
  • Hypolipidemic Agents
  • Lipids
  • Membrane Proteins
  • Membrane Transport Proteins
  • NPC1L1 protein, human
  • Polyethylene Glycols
  • Ezetimibe
  • tyloxapol