Interface chemistry engineering of protein-directed SnO₂ nanocrystal-based anode for lithium-ion batteries with improved performance

Small. 2014 Mar 12;10(5):998-1007. doi: 10.1002/smll.201300843. Epub 2013 Oct 29.

Abstract

A novel uniform amorphous carbon-coated SnO2 nanocrystal (NCs) for use in lithium-ion batteries is formed by utilizing bovine serum albumin (BSA) as both the ligand and carbon source. The SnO2 -carbon composite is then coated by a controlled thickness of polydopamine (PD) layer through in situ polymerization of dopamine. The PD-coated SnO2 -carbon composite is finally mixed with polyacrylic acid (PAA) which is used as binder to accomplish a whole anode system. A crosslink reaction is built between PAA and PD through formation of amide bonds to produce a robust network in the anode system. As a result, the designed electrode exhibits improved reversible capacity of 648 mAh/g at a current density of 100 mA/g after 100 cycles, and an enhanced rate performance of 875, 745, 639, and 523 mAh/g at current densities of 50, 100, 250, and 500 mA/g, respectively. FTIR spectra confirm the formation of crosslink reaction and the stability of the robust network during long-term cycling. The great improvement of capacity and rate performance achieved in this anode system is attributed to two stable interfaces built between the active material (SnO2 -carbon composite) and the buffer layer (PD) and between the buffer layer and the binder (PAA), which effectively diminish the volume change of SnO2 during charge/discharge process and provide a stable matrix for active materials.

Keywords: SnO2 nanocrystals; interfaces; lithium-ion battery.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acrylic Resins
  • Animals
  • Carbon / chemistry
  • Cattle
  • Cross-Linking Reagents / chemistry
  • Electric Power Supplies*
  • Electrochemical Techniques
  • Electrodes
  • Indoles / chemistry
  • Ions
  • Lithium / chemistry*
  • Nanoparticles / chemistry*
  • Nanoparticles / ultrastructure
  • Nanotechnology / methods*
  • Nitrogen / chemistry
  • Polymerization
  • Polymers / chemistry
  • Serum Albumin, Bovine / chemistry*
  • Stress, Mechanical
  • Thermogravimetry
  • Tin Compounds / chemistry*

Substances

  • Acrylic Resins
  • Cross-Linking Reagents
  • Indoles
  • Ions
  • Polymers
  • Tin Compounds
  • polydopamine
  • Serum Albumin, Bovine
  • carbopol 940
  • Carbon
  • Lithium
  • stannic oxide
  • Nitrogen