7-Chloroquinolinotriazoles: synthesis by the azide-alkyne cycloaddition click chemistry, antimalarial activity, cytotoxicity and SAR studies

Eur J Med Chem. 2014 Feb 12:73:295-309. doi: 10.1016/j.ejmech.2013.11.022. Epub 2013 Dec 1.

Abstract

Twenty-seven 7-chloroquinolinotriazole derivatives with different substituents in the triazole moiety were synthesized via copper-catalyzed cycloaddition (CuAAC) click chemistry between 4-azido-7-chloroquinoline and several alkynes. All the synthetic compounds were evaluated for their in vitro activity against Plasmodium falciparum (W2) and cytotoxicity to Hep G2A16 cells. All the products disclosed low cytotoxicity (CC50 > 100 μM) and five of them have shown moderate antimalarial activity (IC50 from 9.6 to 40.9 μM). As chloroquine analogs it was expected that these compounds might inhibit the heme polymerization and SAR studies were performed aiming to explain their antimalarial profile. New structural variations can be designed on the basis of the results obtained.

Keywords: 7-Chloroquinolinotriazoles; Antimalarial activity; Click chemistry; Cytotoxicity in HepG2; Plasmodium falciparum; Quinolines; Triazoles.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkynes / chemistry*
  • Antimalarials / chemical synthesis*
  • Antimalarials / chemistry
  • Antimalarials / pharmacology
  • Antimalarials / toxicity
  • Azides / chemistry*
  • Cell Survival / drug effects
  • Click Chemistry
  • Cycloaddition Reaction
  • Drug Resistance
  • Hep G2 Cells
  • Humans
  • Molecular Structure
  • Plasmodium falciparum / drug effects
  • Plasmodium falciparum / growth & development
  • Structure-Activity Relationship
  • Triazoles / chemical synthesis*
  • Triazoles / chemistry
  • Triazoles / pharmacology
  • Triazoles / toxicity

Substances

  • Alkynes
  • Antimalarials
  • Azides
  • Triazoles