A high-affinity near-infrared fluorescent probe to target bombesin receptors

Mol Imaging Biol. 2014 Oct;16(5):661-9. doi: 10.1007/s11307-014-0727-2.

Abstract

Purpose: This study aimed to create new optical surgical navigation NIRF probes for prostate and breast cancers.

Procedures: IR800-linker-QWAVGHLM-NH2 with linker = GSG, GGG, and G-Abz4 were synthesized and characterized. IC50 for bombesin receptors (BBN-R) in PC-3 prostate and T47D breast cancer cells, fluorescence microscopy in PC-3 cells, and NIRF imaging in mice PC-3 tumor xenografts were studied.

Results: GGG, GSG, and G-Abz4 derivatives had IC50 (nM) for BBN-R+ PC-3 cells = 187 ± 31, 56 ± 5, and 2.6 ± 0.2 and T47D cells = 383 ± 1, 57.4 ± 1.2, and 3.1 ± 1.1, respectively. By microscopy the Abz4 derivative showed the highest uptake, was competed with by BBN, and had little to no binding to BBN-R- cells. In NIRF imaging the G-Abz4 probe was brighter than GGG probe in BBN-R+ tissues in vivo and tissues, tumors, and tumor slices ex vivo. Uptake could be partially blocked in BBN-R+ pancreas but not visibly in tumor.

Conclusions: Linker choice can dominate peptidic BBN-R binding. The G-Abz4 linker yields a higher affinity and specific BBN-R binder in this series of molecules.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Bombesin / chemistry
  • Bombesin / metabolism
  • Cell Line, Tumor
  • Female
  • Fluorescent Dyes* / chemistry
  • Fluorescent Dyes* / pharmacokinetics
  • Humans
  • Inhibitory Concentration 50
  • Mice, Inbred BALB C
  • Mice, Nude
  • Molecular Sequence Data
  • Protein Binding
  • Rats
  • Receptors, Bombesin / metabolism*
  • Spectroscopy, Near-Infrared / methods*
  • Xenograft Model Antitumor Assays

Substances

  • Fluorescent Dyes
  • Receptors, Bombesin
  • Bombesin