Rh(III)-catalyzed cascade oxidative olefination/cyclization of picolinamides and alkenes via C-H activation

Org Lett. 2014 Jun 6;16(11):3142-5. doi: 10.1021/ol501275r. Epub 2014 May 21.

Abstract

Rh(III)-catalyzed cascade oxidative alkenylation/cyclization of picolinamides and alkenes to furnish pyrido pyrrolone derivatives is described, in which three C-H bonds and one N-H bond broke, while one C-C bond and one C-N bond formed. The reaction proceeded with high yield and high regioselectivity and stereoselectivity. Moreover, copper acetate can also be used in catalytic amounts with O2 serving as the terminal oxidant.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkenes / chemistry*
  • Amides / chemical synthesis
  • Amides / chemistry
  • Cyclization
  • Hydrogen Bonding
  • Molecular Structure
  • Oxidation-Reduction
  • Picolinic Acids / chemical synthesis*
  • Picolinic Acids / chemistry*
  • Rhodium
  • Stereoisomerism

Substances

  • Alkenes
  • Amides
  • Picolinic Acids
  • Rhodium
  • picolinamide