Novel inhibitors of enkephalin-degrading enzymes. II: N5'-substituted-4-thioxohydantoic acids as aminopeptidase inhibitors

J Enzyme Inhib. 1989;3(2):103-17. doi: 10.3109/14756368909030369.

Abstract

Some 2-substituted-(2'-aminophenyl)-4-thioxohydantoic acids (o-amino PTC-amino acids) have antinociceptive activity when administered (icv) alone (IC50 = 0.04-0.87 microM/animal) and show a striking prolongation of the antinociceptive action of (D-Ala-2 D-Leu5)-enkephalin (DADL) in combination. The effects are thought to be mediated via opioid receptors since they are naloxone-reversible. Although inhibitors of the enkephalin degrading puromycin-insensitive, bestatin-sensitive aminopeptidase (possibly aminopeptidase M) their action is weak (IC50 = 32 microM leucine, 536 microM, glycine) and they might be considered to have a direct antinociceptive effect on opioid receptors. The titled compounds constitute novel 'lead' compounds for the development of potent aminopeptidase M inhibitors.

MeSH terms

  • Aminopeptidases / antagonists & inhibitors
  • Analgesics*
  • Animals
  • Glycine / analogs & derivatives*
  • Glycine / chemical synthesis
  • Glycine / pharmacology
  • Indicators and Reagents
  • Leucine / analogs & derivatives*
  • Leucine / chemical synthesis
  • Leucine / pharmacology
  • Mice
  • Naloxone / pharmacology
  • Neprilysin / antagonists & inhibitors*
  • Pain / physiopathology*
  • Proline / analogs & derivatives*
  • Proline / chemical synthesis
  • Proline / pharmacology
  • Protease Inhibitors / chemical synthesis*
  • Thiohydantoins / chemical synthesis*
  • Thiohydantoins / pharmacology
  • Thiorphan / pharmacology

Substances

  • Analgesics
  • Indicators and Reagents
  • Protease Inhibitors
  • Thiohydantoins
  • N(5)-(2'-aminophenyl)-4-thioxohydantoic acid
  • 2-(2'-methylpropyl)-N(5)-(2'-aminophenyl)-4-thiohydantoic acid
  • N-(N'-(2'-nitrophenyl)thiocarbamyl)pyrrolidine-2-carboxylic acid
  • Naloxone
  • Proline
  • Thiorphan
  • Aminopeptidases
  • Neprilysin
  • Leucine
  • Glycine