Rapid transfer of transmembrane proteins for single molecule dimerization assays in polymer-supported membranes

ACS Chem Biol. 2014 Nov 21;9(11):2479-84. doi: 10.1021/cb5005806. Epub 2014 Sep 16.

Abstract

Dimerization of transmembrane receptors is a key regulatory factor in cellular communication, which has remained challenging to study under well-defined conditions in vitro. We developed a novel strategy to explore membrane protein interactions in a controlled lipid environment requiring minute sample quantities. By rapid transfer of transmembrane proteins from mammalian cells into polymer-supported membranes, membrane proteins could be efficiently fluorescence labeled and reconstituted with very low background. Thus, differential ligand-induced dimerization of the type I interferon (IFN) receptor subunits IFNAR1 and IFNAR2 could be probed quantitatively at physiologically relevant concentrations by single molecule imaging. These measurements clearly support a regulatory role of the affinity of IFNs toward IFNAR1 for controlling the level of receptor dimerization.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Dimerization
  • Ligands
  • Mammals
  • Membrane Proteins / chemistry*
  • Polymers / chemistry*

Substances

  • Ligands
  • Membrane Proteins
  • Polymers