Formal [4+2] annulation of enaminones and cyanomethyl sulfur ylide: one-pot access to polysubstituted pyridin-2(1H)-ones

Chem Commun (Camb). 2014 Dec 18;50(97):15378-80. doi: 10.1039/c4cc06665k. Epub 2014 Oct 28.

Abstract

A facile and efficient one-pot synthesis of polysubstituted pyridin-2(1H)-ones from readily available enaminones and the cyanomethyl sulfonium bromide salt in the presence of cesium carbonate is developed, and a mechanism involving sequential nucleophilic vinylic substitution (S(N)V), intramolecular nucleophilic cyclization and dealkylation reactions is proposed.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amides / chemistry
  • Bromides / chemistry
  • Carbonates / chemistry
  • Cesium / chemistry
  • Cyclization
  • Dimethyl Sulfoxide / chemistry
  • Pyridones / chemical synthesis*

Substances

  • Amides
  • Bromides
  • Carbonates
  • Pyridones
  • Cesium
  • cesium carbonate
  • Dimethyl Sulfoxide