Tumor microenvironment sensitive doxorubicin delivery and release to glioma using angiopep-2 decorated gold nanoparticles

Biomaterials. 2015 Jan:37:425-35. doi: 10.1016/j.biomaterials.2014.10.007. Epub 2014 Oct 29.

Abstract

Glioma is still hard to be treated due to their complex microenvironment. In this study, a gold nanoparticle-based delivery system was developed. The system, An-PEG-DOX-AuNPs, was loaded with doxorubicin (DOX) through hydrazone, an acid-responsive linker, and was functionalized with angiopep-2, a specific ligand of low density lipoprotein receptor-related protein-1 (LRP1), which could mediate the system to penetrate blood brain barrier and target to glioma cells. The particle size of An-PEG-DOX-AuNPs was 39.9 nm with a zeta potential of -19.3 mV, while the DOX loading capacity was 9.7%. In vitro, the release of DOX from DOX-AuNPs was pH-dependent. At lower pH values, especially 5.0 and 6.0, release of DOX was much quicker than that at pH 6.8 and 7.4. After coating with PEG, the acid-responsive release of DOX from PEG-DOX-AuNPs was almost the same as that from DOX-AuNPs. Cellular uptake study showed obviously higher intensity of intracellular An-PEG-DOX-AuNPs compared with PEG-DOX-AuNPs. In vivo, An-PEG-DOX-AuNPs could distribute into glioma at a higher intensity than that of PEG-DOX-AuNPs and free DOX. Correspondingly, glioma-bearing mice treated with An-PEG-DOX-AuNPs displayed the longest median survival time, which was 2.89-fold longer than that of saline. In conclusion, An-PEG-DOX-AuNPs could specifically deliver and release DOX in glioma and significantly expand the median survival time of glioma-bearing mice.

Keywords: Doxorubicin; Glioma; Gold nanoparticles; Sensitive release; Tumor microenvironment.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Brain Neoplasms / drug therapy*
  • Brain Neoplasms / pathology
  • Doxorubicin / chemistry
  • Doxorubicin / pharmacology
  • Doxorubicin / therapeutic use*
  • Drug Delivery Systems*
  • Endosomes / drug effects
  • Endosomes / metabolism
  • Glioma / drug therapy*
  • Glioma / pathology
  • Gold / chemistry*
  • Male
  • Metal Nanoparticles / ultrastructure
  • Mice
  • Peptides / pharmacology
  • Peptides / therapeutic use*
  • Polyethylene Glycols / chemistry
  • Proton Magnetic Resonance Spectroscopy
  • Rats
  • Subcellular Fractions / drug effects
  • Subcellular Fractions / metabolism
  • Tissue Distribution / drug effects
  • Tumor Microenvironment* / drug effects

Substances

  • Angiopep-2
  • Peptides
  • Polyethylene Glycols
  • Gold
  • Doxorubicin