Synthesis and structure-activity relationships of novel phenoxyacetamide inhibitors of the Pseudomonas aeruginosa type III secretion system (T3SS)

Bioorg Med Chem. 2015 Mar 1;23(5):1027-43. doi: 10.1016/j.bmc.2015.01.011. Epub 2015 Jan 13.

Abstract

The increasing prevalence of drug-resistant bacterial infections is driving the discovery and development not only of new antibiotics, but also of inhibitors of virulence factors that are crucial for in vivo pathogenicity. One such virulence factor is the type III secretion system (T3SS), which plays a critical role in the establishment and dissemination of Pseudomonas aeruginosa infections. We have recently described the discovery and characterization of a series of inhibitors of P. aeruginosa T3SS based on a phenoxyacetamide scaffold. To better characterize the factors involved in potent T3SS inhibition, we have conducted a systematic exploration of this structure, revealing several highly responsive structure-activity relationships indicative of interaction with a specific target. Most of the structural features contributing to potency were additive, and combination of those features produced optimized inhibitors with IC50 values <1μM.

Keywords: Mitsunobu reaction; Phenoxyacetamide; Pseudomonas aeruginosa; Type III secretion system; Virulence factor.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Acetates / chemistry
  • Acetates / pharmacology*
  • Amides / chemistry
  • Animals
  • Anti-Bacterial Agents / pharmacology*
  • CHO Cells
  • Cricetinae
  • Cricetulus
  • Pseudomonas aeruginosa / drug effects*
  • Pseudomonas aeruginosa / metabolism
  • Structure-Activity Relationship

Substances

  • Acetates
  • Amides
  • Anti-Bacterial Agents
  • phenoxyacetic acid