Small-molecule inhibitors of ERK-mediated immediate early gene expression and proliferation of melanoma cells expressing mutated BRaf

Biochem J. 2015 May 1;467(3):425-38. doi: 10.1042/BJ20131571.

Abstract

Constitutive activation of the extracellular-signal-regulated kinases 1 and 2 (ERK1/2) are central to regulating the proliferation and survival of many cancer cells. The current inhibitors of ERK1/2 target ATP binding or the catalytic site and are therefore limited in their utility for elucidating the complex biological roles of ERK1/2 through its phosphorylation and regulation of over 100 substrate proteins. To overcome this limitation, a combination of computational and experimental methods was used to identify low-molecular-mass inhibitors that are intended to target ERK1/2 substrate-docking domains and selectively interfere with ERK1/2 regulation of substrate proteins. In the present study, we report the identification and characterization of compounds with a thienyl benzenesulfonate scaffold that were designed to inhibit ERK1/2 substrates containing an F-site or DEF (docking site for ERK, FXF) motif. Experimental evidence shows the compounds inhibit the expression of F-site containing immediate early genes (IEGs) of the Fos family, including c-Fos and Fra1, and transcriptional regulation of the activator protein-1 (AP-1) complex. Moreover, this class of compounds selectively induces apoptosis in melanoma cells containing mutated BRaf and constitutively active ERK1/2 signalling, including melanoma cells that are inherently resistant to clinically relevant kinase inhibitors. These findings represent the identification and initial characterization of a novel class of compounds that inhibit ERK1/2 signalling functions and their potential utility for elucidating ERK1/2 and other signalling events that control the growth and survival of cancer cells containing elevated ERK1/2 activity.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology
  • Cell Line, Tumor
  • Cell Proliferation / drug effects
  • Cell Proliferation / genetics
  • Computer Simulation
  • Drug Design
  • Drug Screening Assays, Antitumor
  • Gene Expression / drug effects
  • Genes, Immediate-Early / drug effects*
  • HeLa Cells
  • Humans
  • Jurkat Cells
  • Ligands
  • MAP Kinase Signaling System / drug effects*
  • MAP Kinase Signaling System / genetics
  • Melanoma / drug therapy*
  • Melanoma / genetics
  • Melanoma / pathology
  • Models, Molecular
  • Molecular Dynamics Simulation
  • Mutation
  • Phosphorylation
  • Promoter Regions, Genetic / drug effects
  • Protein Kinase Inhibitors / chemistry
  • Protein Kinase Inhibitors / pharmacology
  • Proto-Oncogene Proteins B-raf / genetics*
  • Proto-Oncogene Proteins c-fos / chemistry
  • Proto-Oncogene Proteins c-fos / metabolism
  • Serum Response Element
  • Transcription Factor AP-1 / genetics

Substances

  • Antineoplastic Agents
  • Ligands
  • Protein Kinase Inhibitors
  • Proto-Oncogene Proteins c-fos
  • Transcription Factor AP-1
  • BRAF protein, human
  • Proto-Oncogene Proteins B-raf