Discovery of potent and selective 8-fluorotriazolopyridine c-Met inhibitors

J Med Chem. 2015 Mar 12;58(5):2417-30. doi: 10.1021/jm501913a. Epub 2015 Mar 3.

Abstract

The overexpression of c-Met and/or hepatocyte growth factor (HGF), the amplification of the MET gene, and mutations in the c-Met kinase domain can activate signaling pathways that contribute to cancer progression by enabling tumor cell proliferation, survival, invasion, and metastasis. Herein, we report the discovery of 8-fluorotriazolopyridines as inhibitors of c-Met activity. Optimization of the 8-fluorotriazolopyridine scaffold through the combination of structure-based drug design, SAR studies, and metabolite identification provided potent (cellular IC50 < 10 nM), selective inhibitors of c-Met with desirable pharmacokinetic properties that demonstrate potent inhibition of HGF-mediated c-Met phosphorylation in a mouse liver pharmacodynamic model.

MeSH terms

  • Animals
  • Cell Proliferation / drug effects
  • Drug Design
  • Drug Discovery*
  • Hepatocyte Growth Factor / metabolism
  • Humans
  • Male
  • Mice
  • Microsomes, Liver / drug effects
  • Models, Molecular
  • Molecular Structure
  • Phosphorylation / drug effects
  • Prostatic Neoplasms / drug therapy*
  • Prostatic Neoplasms / pathology
  • Protein Kinase Inhibitors / chemistry
  • Protein Kinase Inhibitors / pharmacokinetics
  • Protein Kinase Inhibitors / pharmacology*
  • Proto-Oncogene Proteins c-met / antagonists & inhibitors*
  • Quinolines / chemistry
  • Quinolines / pharmacokinetics
  • Quinolines / pharmacology*
  • Rats
  • Rats, Sprague-Dawley
  • Signal Transduction / drug effects
  • Tissue Distribution
  • Triazoles / chemistry
  • Triazoles / pharmacokinetics
  • Triazoles / pharmacology*
  • Xenograft Model Antitumor Assays

Substances

  • 5-(8-fluoro-3-(1-(3-(2-methoxyethoxy)quinolin-6-yl)ethyl)(1,2,4)triazolo(4,3-a)pyridin-6-yl)-3-methylisoxazole
  • Protein Kinase Inhibitors
  • Quinolines
  • Triazoles
  • Hepatocyte Growth Factor
  • Proto-Oncogene Proteins c-met