Half-life extension of the HIV-fusion inhibitor peptide TRI-1144 using a novel linker technology

Eur J Pharm Biopharm. 2015 Jun:93:254-9. doi: 10.1016/j.ejpb.2015.04.003. Epub 2015 Apr 18.

Abstract

We have previously developed a linker technology for half-life extension of peptides, proteins and small molecule drugs (1). The linkers undergo β-elimination reactions with predictable cleavage rates to release the native drug. Here we utilize this technology for half-life extension of the 38 amino acid HIV-1 fusion inhibitor TRI-1144. Conjugation of TRI-1144 to 40 kDa PEG by an appropriate β-eliminative linker and i.v. administration of the conjugate increased the in vivo half-life of the released peptide from 4 to 34 h in the rat, and the pharmacokinetic parameters were in excellent accord with a one-compartment model. From these data we simulated the pharmacokinetics of the PEG-TRI-1144 conjugate in humans, predicting a t1/2,β of 70 h for the released peptide, and that a serum concentration of 25 nM could be maintained by weekly doses of 8 μmol of the conjugate. Using a non-circulating carrier (2) similar simulations indicated a t1/2,β of 150 h for the peptide released from the conjugate and that dosing of only 1.8 μmol/week could maintain serum concentrations of TRI-1144 above 25 nM. Hence, releasable β-eliminative linkers provide significant half-life extension to TRI-1144 and would be expected to do likewise for related peptides.

Keywords: Combination therapy; Drug delivery; Half-life extension; Pegylation; Peptide drugs; Prodrug.

MeSH terms

  • Administration, Intravenous
  • Animals
  • Chemistry, Pharmaceutical
  • Computer Simulation
  • HIV Envelope Protein gp41 / administration & dosage
  • HIV Envelope Protein gp41 / blood
  • HIV Envelope Protein gp41 / chemical synthesis
  • HIV Envelope Protein gp41 / pharmacokinetics*
  • HIV Fusion Inhibitors / administration & dosage
  • HIV Fusion Inhibitors / blood
  • HIV Fusion Inhibitors / chemical synthesis
  • HIV Fusion Inhibitors / pharmacokinetics*
  • Half-Life
  • Hydrolysis
  • Male
  • Metabolic Clearance Rate
  • Models, Biological
  • Peptide Fragments / administration & dosage
  • Peptide Fragments / blood
  • Peptide Fragments / chemical synthesis
  • Peptide Fragments / pharmacokinetics*
  • Peptides
  • Polyethylene Glycols / administration & dosage
  • Polyethylene Glycols / chemical synthesis
  • Polyethylene Glycols / pharmacokinetics*
  • Prodrugs / administration & dosage
  • Prodrugs / chemical synthesis
  • Prodrugs / pharmacokinetics*
  • Rats, Sprague-Dawley
  • Technology, Pharmaceutical / methods

Substances

  • HIV Envelope Protein gp41
  • HIV Fusion Inhibitors
  • Peptide Fragments
  • Peptides
  • Prodrugs
  • T2635 peptide
  • Polyethylene Glycols