Cloning, expression, and characterization of a thermostable l-arginase from Geobacillus thermodenitrificans NG80-2 for l-ornithine production

Biotechnol Appl Biochem. 2016 May;63(3):391-7. doi: 10.1002/bab.1385. Epub 2015 Jun 24.

Abstract

Arginase (l-arginine amidinohydrolase, EC 3.5.3.1) can efficiently catalyze conversion of arginine to ornithine. Therefore, this enzyme can be used to produce l-ornithine from l-arginine. In this article, the l-arginase gene encoding the Geobacillus thermodenitrificans NG80-2 was cloned and overexpressed in Escherichia coli. The specific activity of the purified enzyme was 138.3 U/mg. The molecular mass of the l-arginase was approximately 33.0 kDa as estimated by SDS-PAGE and 192.0 kDa as determined by gel-filtration chromatography. Manganese ions were the optimum metal cofactor for activity, whereas the enzyme was slightly inhibited by Mg(2+) , Cu(2+) , Ba(2+) , Ca(2+) , and Zn(2+) . Activity was optimal at pH 9.0 and 80 °C, and the protein was stable at 40 and 50 °C. The recombinant enzyme was a uricotelic arginase. Using arginine as the substrate, the Michaelis-Menten constant (Km ) and catalytic efficiency (kcat /Km ) were measured to be 171.9 mM and 3.8 mM(-1) s(-1) , respectively. Trp and His residues were directly involved in the l-arginase activity evaluated by inactivation agents. The biosynthesis yield of l-ornithine by the purified enzyme was 36.9 g/L, and the molar yield was 97.2%.

Keywords: Geobacillus thermodenitrificans; biocatalysis; gene expression; l-arginase; l-arginine; l-ornithine.

MeSH terms

  • Amino Acid Sequence
  • Arginase / chemistry
  • Arginase / genetics*
  • Arginase / isolation & purification
  • Arginase / metabolism*
  • Enzyme Activation
  • Enzyme Stability
  • Feasibility Studies
  • Gene Expression
  • Geobacillus / enzymology*
  • Geobacillus / genetics
  • Hydrogen-Ion Concentration
  • Kinetics
  • Metals / pharmacology
  • Molecular Weight
  • Ornithine / biosynthesis*
  • Sequence Analysis, DNA
  • Temperature*

Substances

  • Metals
  • Ornithine
  • Arginase