Polymorphism-Dependent Spin-Crossover: Hysteretic Two-Step Spin Transition with an Ordered [HS-HS-LS] Intermediate Phase

Inorg Chem. 2015 Jun 1;54(11):5145-7. doi: 10.1021/acs.inorgchem.5b00629. Epub 2015 May 8.

Abstract

A mononuclear iron(II) complex has been isolated in two polymorphs. Polymorph 1b remains high-spin over all temperatures, whereas polymorph 1a undergoes a cooperative two-step spin crossover accompanied by symmetry breaking, showing an ordered 2:1 high-spin-low-spin intermediate phase.