Effects of blood processing and sample storage on the stability of biotherapeutics and anti-drug antibodies

Bioanalysis. 2015;7(11):1325-35. doi: 10.4155/bio.15.66.

Abstract

Background: Pre-analytical factors such as sample processing, handling or storage could affect the stability of biotherapeutics and anti-drug antibodies in clinical samples, potentially impacting the pharmacokinetic and immunogenicity assessments.

Methods: We used sarilumab, a fully human IgG1 monoclonal antibody, and evaluated the stability of sarilumab (both functional and bound forms) and anti-sarilumab antibodies in blood samples during serum collection and the impact of various processing conditions on the analyte stability in serum for long-term storage. We also assessed the incurred sample stability of these analytes in samples from clinical studies.

Conclusion: Assessment of analyte stability can provide relevant information about sample stability under different pre-analytical conditions and improve the confidence in the validity of bioanalytical data generated.

MeSH terms

  • Animals
  • Antibodies / immunology*
  • Antibodies, Monoclonal, Humanized / blood*
  • Antibodies, Monoclonal, Humanized / immunology*
  • Antibodies, Monoclonal, Humanized / metabolism
  • Blood Preservation / methods
  • Blood Specimen Collection / methods
  • Drug Stability
  • Female
  • Humans
  • Immunoassay / methods
  • Luminescent Measurements / methods
  • Male
  • Protein Stability
  • Serum / immunology
  • Serum / metabolism

Substances

  • Antibodies
  • Antibodies, Monoclonal, Humanized
  • sarilumab