Isoprene Polymerization on Iron Nanoparticles Confined in Carbon Nanotubes

Chemistry. 2015 Nov 23;21(48):17437-44. doi: 10.1002/chem.201501165. Epub 2015 Oct 16.

Abstract

The confinement of air-protected metallic magnetic nanoparticles in the inner cavity of carbon nanotubes (CNTs) should offer an interesting perspective for biomedical applications or for controlling CNT alignment in composites. Because the direct confinement of polymer-precoated nanoparticles in CNTs could be restricted by diffusion limitations, we developed a process based on: 1) the confinement of iron nanoparticles surface-modified with an iron polymerization catalyst in the cavity of CNTs and 2) the polymerization of isoprene on the confined nanoparticles. The resulting material consists in CNT-confined iron nanoparticles coated with a polyisoprene air barrier. This approach constitutes a proof of concept for the development of smart materials for use in medicine or composites.

Keywords: carbon; iron; magnetic properties; nanoparticles; nanotubes; polymerization.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Butadienes / chemistry*
  • Catalysis
  • Hemiterpenes / chemistry*
  • Iron / chemistry*
  • Magnetics
  • Metal Nanoparticles / chemistry*
  • Nanotubes, Carbon / chemistry*
  • Pentanes / chemistry*
  • Polymerization

Substances

  • Butadienes
  • Hemiterpenes
  • Nanotubes, Carbon
  • Pentanes
  • isoprene
  • Iron