Structural studies on the fucosamine-containing O-specific polysaccharide of Proteus vulgaris O19

Eur J Biochem. 1989 Mar 1;180(1):95-9. doi: 10.1111/j.1432-1033.1989.tb14619.x.

Abstract

The polysaccharide chain of Proteus vulgaris O19 lipopolysaccharide contains D-galactose, N-acetyl-D-glucosamine N-acetyl-D-galactosamine and N-acetyl-L-fucosamine in the ratio 1:1:1:1. The structure of the polysaccharide was established by full acid hydrolysis and methylation analysis, as well as by non-destructive methods, i.e. the computer-assisted evaluation of the 13C-NMR spectrum and computer-assisted evaluation of the specific optical rotation by Klyne's rule. The polysaccharide is regular and built up of tetrasaccharide repeating units of the following structure: ----3)-alpha-L-FucNAcp-(1----3)-beta-D-GlcNAcp-(1----3)-alph a-D-Galp- (1----4)-alpha-D-GalNAcp-(1---- The O19-antiserum cross-reacts with lipopolysaccharide from P. vulgaris O42, the structure of which is still unknown. No cross-reactions were observed with O-polysaccharides Pseudomonas aeruginosa O7 and Salmonella arizonae O59 in spite of some structural similarities.

MeSH terms

  • Acetylgalactosamine / analysis*
  • Acetylglucosamine / analysis*
  • Blotting, Western
  • Carbohydrate Conformation
  • Electrophoresis, Polyacrylamide Gel
  • Fucose / analogs & derivatives*
  • Fucose / analysis
  • Fucose / immunology
  • Galactosamine / analogs & derivatives*
  • Galactose / analysis*
  • Glucosamine / analogs & derivatives*
  • Hydrolysis
  • Immune Sera
  • Lipopolysaccharides / analysis*
  • Magnetic Resonance Spectroscopy
  • Methylation
  • Molecular Structure
  • Optical Rotation
  • Precipitin Tests
  • Proteus vulgaris / analysis*

Substances

  • Immune Sera
  • Lipopolysaccharides
  • Fucose
  • N-acetylfucosamine
  • Galactosamine
  • Acetylgalactosamine
  • Glucosamine
  • Acetylglucosamine
  • Galactose