Total Synthesis and Tentative Structural Elucidation of Cryptomoscatone E3: Interplay of Experimental and Computational Studies

J Org Chem. 2015 Dec 18;80(24):12027-37. doi: 10.1021/acs.joc.5b01956. Epub 2015 Nov 18.

Abstract

A successful combination of computational chemistry and total synthesis was explored to tentatively elucidate the absolute configuration of cryptomoscatone E3, a polyketide isolated from the Brazilian tree Cryptocarya mandiocanna. Two independent synthetic approaches are discussed based on asymmetric allylation, ring closing metathesis, and aldol reactions.

Publication types

  • Research Support, Non-U.S. Gov't