A miniature closed-circle flow cell for high photon flux X-ray scattering experiments

J Synchrotron Radiat. 2015 Nov;22(6):1555-8. doi: 10.1107/S1600577515016331. Epub 2015 Sep 29.

Abstract

A closed-circle miniature flow cell for high X-ray photon flux experiments on radiation-sensitive liquid samples is presented. The compact cell is made from highly inert material and the flow is induced by a rotating magnetic stir bar, which acts as a centrifugal pump inside the cell. The cell is ideal for radiation-sensitive yet precious or hazardous liquid samples, such as concentrated acids or bases. As a demonstration of the cell's capabilities, X-ray Raman scattering spectroscopy data on the oxygen K-edge of liquid water under ambient conditions are presented.

Keywords: inelastic X-ray scattering; liquids; radiation damage; sample environments.