Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetra-hydro-naphthalen-1-yl-idene]amino}-thio-urea

Joel T Mague; Shaaban K Mohamed; Mehmet Akkurt; Alaa A Hassan; Ahmed T Abdel-Aziz; Mustafa R Albayati

doi:10.1107/S2056989015021076

Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetra-hydro-naphthalen-1-yl-idene]amino}-thio-urea

Acta Crystallogr E Crystallogr Commun. 2015 Nov 21;71(Pt 12):o976-7. doi: 10.1107/S2056989015021076. eCollection 2015 Dec 1.

Authors

Joel T Mague¹, Shaaban K Mohamed², Mehmet Akkurt³, Alaa A Hassan⁴, Ahmed T Abdel-Aziz⁴, Mustafa R Albayati⁵

Affiliations

¹ Department of Chemistry, Tulane University, New Orleans, LA 70118, USA.
² Faculty of Science & Engineering, School of Healthcare Science, Manchester Metropolitan University, Manchester M1 5GD, England; Chemistry Department, Faculty of Science, Minia University, 61519 El-Minia, Egypt.
³ Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.
⁴ Chemistry Department, Faculty of Science, Minia University, 61519 El-Minia, Egypt.
⁵ Kirkuk University, College of Education, Department of Chemistry, Kirkuk, Iraq.

Abstract

In the title compound, C14H17N3S, the dihedral angle between the planes of the benzene ring and the thio-semicarbazone group (r.m.s. deviation = 0.031 Å) is 8.45 (4)°. A short intra-molcular N-H⋯N contact is seen. In the crystal, weak N-H⋯S hydrogen bonds connect the mol-ecules into C(4) chains propagating in the [010] direction, with adjacent mol-ecules in the chain related by 21 screw-axis symmetry.

Keywords: N—H⋯S hydrogen bond; crystal structure; thiosemicarbazone.