Steroid hormone profiles plus α-fetoprotein for diagnosing primary liver cancer by liquid chromatography tandem mass spectrometry

Clin Chim Acta. 2016 Jun 1:457:92-8. doi: 10.1016/j.cca.2016.03.022. Epub 2016 Apr 6.

Abstract

Background: Primary liver cancer (PLC) is one of the most common malignant tumors world-wide but its pathogenesis is unclear. We suggest that steroid hormones may offer diagnostic information for PLC.

Methods: Using liquid chromatography (UPLC) and tandem mass spectrometry (MS/MS), we quantified 7 endogenous steroids in 66 PLC human serum samples, 59 liver cirrhosis (LC) samples, and 65 healthy volunteers (HV). Data were assessed chemometrically and with Mann-Whitney U tests and partial least squares discriminant analysis (PLS-DA).

Results: For PLC patients, androgens were low and estrogen was high. PLS-DA analysis discriminated between healthy subjects and cancer patients using (estrone+estradiol)/testosterone ratios. Moreover, cirrhosis patients were also distinguished with receiver operating characteristic curves indicating the specificity and sensitivity of our current approach.

Conclusions: Steroid hormone profiling by UPLC-MS/MS may be promising for early diagnosis of PLC but investigations with more patients and steroids are required to confirm the utility of these biomarkers for clinical applications.

Keywords: Biomarkers; Human serum; Primary liver cancer; Steroid hormones; UPLC-MS/MS.

Publication types

  • Validation Study

MeSH terms

  • Androgens / metabolism*
  • Chromatography, Liquid / methods*
  • Estrogens / metabolism*
  • Humans
  • Limit of Detection
  • Liver Neoplasms / diagnosis*
  • Reproducibility of Results
  • Tandem Mass Spectrometry / methods*
  • alpha-Fetoproteins / metabolism*

Substances

  • Androgens
  • Estrogens
  • alpha-Fetoproteins