Impact of anti-PEG IgM antibodies on the pharmacokinetics of pegylated asparaginase preparations in mice

Eur J Pharm Sci. 2016 Aug 25:91:122-30. doi: 10.1016/j.ejps.2016.06.007. Epub 2016 Jun 10.

Abstract

The potential impact of pre-existing anti-PEG antibodies on the asparaginase activity kinetics of two pegylated l-asparaginase preparations - pegylated recombinant l-asparaginase (PEG-rASNase MC0609) and pegaspargase (pegylated Escherichia colil-asparaginase) - was investigated in immune competent, naïve B6D2F1-hybrid mice. To generate anti-PEG antibodies, mice were pre-sensitised by repeated injections of 40kDa PEG-Diol without being conjugated to a carrier. Successful PEG-Diol pre-sensitisation was verified by analysis of anti-PEG antibody titers in serum. 88-100% of animals developed PEG-specific anti-PEG IgM antibodies after PEG-Diol pre-sensitisation. All animals positive for anti-PEG IgM antibodies and control animals (without prior PEG-Diol pre-sensitisation) were treated once with PEG-rASNase MC0609 or pegaspargase, and asparaginase enzyme activity levels and immunogenicity of both preparations were analysed. Known serum asparaginase activity profiles were measured after treatment with PEG-rASNase MC0609 or pegaspargase in all treatment groups. No rapid decrease of asparaginase activity was observed - irrespective of successful PEG-Diol pre-sensitisation and presence of acquired anti-drug-IgG and/or anti-PEG IgM antibodies. In conclusion, the pharmacokinetics of pegylated l-asparaginase was unaffected by the presence of pre-existing anti-PEG IgM antibodies in immune competent B6D2F1-hybrid mice Probably the titre or affinity of these anti-PEG IgM antibodies were too low to influence the pharmacokinetics of PEG-rASNase MC0609 or pegaspargase or anti-PEG IgM antibodies bound to PEG-ASNase without neutralising capabilities. Thus, early loss of asparaginase activity as observed in serum of ALL patients is a complex process and cannot be explained solely by the existence of pre-existing anti-PEG antibodies.

Keywords: Anti-PEG antibodies; Immunogenicity; Mouse; PEGylation; Pharmacokinetics; l-asparaginase.

MeSH terms

  • Animals
  • Antineoplastic Agents* / blood
  • Antineoplastic Agents* / immunology
  • Antineoplastic Agents* / pharmacokinetics
  • Asparaginase* / antagonists & inhibitors
  • Asparaginase* / blood
  • Asparaginase* / immunology
  • Asparaginase* / pharmacokinetics
  • Female
  • Immunoglobulin G / blood*
  • Immunoglobulin G / immunology
  • Immunoglobulin M / blood*
  • Immunoglobulin M / immunology
  • Mice
  • Polyethylene Glycols* / pharmacokinetics
  • Recombinant Proteins / blood
  • Recombinant Proteins / immunology
  • Recombinant Proteins / pharmacokinetics

Substances

  • Antineoplastic Agents
  • Immunoglobulin G
  • Immunoglobulin M
  • Recombinant Proteins
  • Polyethylene Glycols
  • pegaspargase
  • Asparaginase