Combined QSAR-based virtual screening and fluorescence binding assay to identify natural product mediators of Interferon Regulatory Factor 7 (IRF-7) in pulmonary infection

SAR QSAR Environ Res. 2016 Nov;27(11):967-976. doi: 10.1080/1062936X.2016.1243576. Epub 2016 Oct 20.

Abstract

Interferon regulatory factor-7 (IRF-7) is involved in pulmonary infection and pneumonia. Here, a synthetic strategy that combined quantitative structure-activity relationship (QSAR)-based virtual screening and in vitro binding assay was described to identify new and potent mediator ligands of IRF-7 from natural products. In the procedure, a QSAR scoring function was developed and validated using Gaussian process (GP) regression and a structure-based set of protein-ligand affinity data. By integrating hotspot pocket prediction, pharmacokinetics profile analysis and molecular docking calculations, the scoring function was successfully applied to virtual screening against a large library of structurally diverse, drug-like natural products. With the method we were able to identify a number of potential hits, from which several compounds were found to have moderate or high affinity to IRF-7 using fluorescence binding assays, with dissociation constants Kd at micromolar level. We have also examined the structural basis and noncovalent interactions of computationally modelled IRF-7 complex with its potent ligands. It is revealed that hydrophobic forces and van der Waals contacts play a central role in stabilization of the complex architecture, while few hydrogen bonds confer additional specificity for the protein-ligand recognition.

Keywords: Interferon regulatory factor-7; natural product; pneumonia; pulmonary infection; quantitative structure–activity relationship.

MeSH terms

  • Biological Products / chemistry*
  • Biological Products / pharmacology
  • Fluorescence
  • Hydrogen Bonding
  • Hydrophobic and Hydrophilic Interactions
  • Interferon Regulatory Factor-7 / metabolism*
  • Ligands
  • Molecular Docking Simulation
  • Protein Binding
  • Quantitative Structure-Activity Relationship*
  • Respiratory Tract Infections / drug therapy
  • Respiratory Tract Infections / metabolism*

Substances

  • Biological Products
  • Interferon Regulatory Factor-7
  • Ligands