An Asymmetric Conformational Change in LacY

Biochemistry. 2017 Apr 4;56(13):1943-1950. doi: 10.1021/acs.biochem.7b00134. Epub 2017 Mar 23.

Abstract

Galactoside/H+ symport by the lactose permease of Escherichia coli (LacY) involves reciprocal opening and closing of periplasmic and cytoplasmic cavities so that sugar- and H+-binding sites become alternatively accessible to either side of the membrane. After reconstitution into proteoliposomes, LacY with the periplasmic cavity sealed by cross-linking paired-Cys residues does not bind sugar from the periplasmic side. However, reduction of the S-S bond restores opening of the periplasmic cavity and galactoside binding. Furthermore, nanobodies that stabilize the double-Cys mutant in a periplasmic-open conformation and allow free access of galactoside to the binding site do so only after reduction of the S-S bond. In contrast, when cross-linked LacY is solubilized in detergent, galactoside binding is observed, indicating that the cytoplasmic cavity is patent. Sugar binding from the cytoplasmic side exhibits nonlinear stopped-flow kinetics, and analysis reveals a two-step process in which a conformational change precedes binding. Because the cytoplasmic cavity is spontaneously closing and opening in the symporter with a sealed periplasmic cavity, it is apparent that an asymmetrical conformational transition controls access of sugar to the binding site.

MeSH terms

  • Binding Sites
  • Biological Transport
  • Cysteine / chemistry*
  • Disulfides / chemistry*
  • Escherichia coli / chemistry
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Escherichia coli Proteins / chemistry*
  • Escherichia coli Proteins / metabolism
  • Galactose / chemistry*
  • Galactose / metabolism
  • Gene Expression
  • Kinetics
  • Models, Molecular
  • Monosaccharide Transport Proteins / chemistry*
  • Monosaccharide Transport Proteins / metabolism
  • Oxidation-Reduction
  • Protein Binding
  • Protein Domains
  • Protein Structure, Secondary
  • Proteolipids / chemistry*
  • Proteolipids / metabolism
  • Protons*
  • Symporters / chemistry*
  • Symporters / metabolism
  • Thermodynamics

Substances

  • Disulfides
  • Escherichia coli Proteins
  • LacY protein, E coli
  • Monosaccharide Transport Proteins
  • Proteolipids
  • Protons
  • Symporters
  • proteoliposomes
  • Cysteine
  • Galactose