Selective construction of quaternary stereocentres in radical cyclisation cascades triggered by electron-transfer reduction of amide-type carbonyls

Org Biomol Chem. 2017 May 16;15(19):4159-4164. doi: 10.1039/c7ob00739f.

Abstract

Radical-radical cyclisation cascades, triggered by single-electron-transfer to amide-type carbonyls using SmI2-H2O-LiBr, result in the selective construction of quaternary carbon stereocentres. The cascades deliver tricyclic barbiturates with four stereocentres in good yield and with excellent diastereocontrol.